BT

Typical G.C. analysis

abies balsamea needle oil canada
#%LeftshiftComponents
240.31-2.07  borneol
194.89-16.22  bornyl acetate
250.02-0.21delta- cadinene
53.49-9.72  camphene
180.04-0.56  camphor
80.00-27.27delta-3- carene
200.00-0.27alpha- cedrene
150.03-0.16para- cymene
220.06-0.60alpha- humulene
121.83-15.63  limonene
100.71-2.28  myrcene
170.00-0.691- octen-1-yl acetate
90.03-0.19alpha- phellandrene
134.39-12.64beta- phellandrene
46.18-14.29alpha- pinene
628.10-56.10beta- pinene
70.02-0.23  sabinene
10.30-1.41  santene
210.06-0.29  terpinen-4-ol
110.02-0.11alpha- terpinene
140.06-0.31gamma- terpinene
230.56-4.48alpha- terpineol
160.17-1.68  terpinolene
30.00-0.21alpha- thujene
260.00-2.89  thymol
20.56-1.69  tricyclene

J. M. Regimbal and G. Collin, Essential Oil Analysis of Balsam Fir Abies balsamea (L.) Mill. J. Essent. Oil Res., 6, 229-238 (1994).

P&F 20, No. 5, 95, (1995)

fir needle oil siberian
#%LeftshiftComponents
171.66  borneol
1830.96  bornyl acetate
424.27  camphene
160.05  camphor
812.23delta-3- carene
200.59beta- caryophyllene
100.15para- cymene
190.17  geranyl acetate
210.33alpha- humulene
124.08  limonene
60.69  myrcene
70.12alpha- phellandrene
112.47beta- phellandrene
313.74alpha- pinene
51.57beta- pinene
12.52  santene
150.14  terpinen-4-ol
90.10alpha- terpinene
130.14gamma- terpinene
141.12  terpinolene
22.38  tricyclene

A. Orav, K. Kuningas and T. Kailas, Computerized capillary gas chromatographic identification and determination of Siberian fir oil constituents. J. Chromatogr., A, 697, 495-499 (1995).

P&F 21, No. 6, 55, (1996)

pinus mugo turra var. pumilio (haenke) zenari oil
#%LeftshiftComponents
36trace  bisabolol
230.43  bornyl acetate
200.13beta- bourbonene
3111.89delta-cadinene + geranyl acetate
375.82alpha- cadinol
342.17T- cadinol
320.13  calamenene
45.24  camphene
711.77delta-3- carene
260.40beta- caryophyllene
190.62alpha- copaene
180.33alpha- cubebene
140.09para- cymene
254.81beta- elemene
297.62  germacrene D
17trace(Z)-3- hexen-1-yl acetate
270.86alpha- humulene
109.13  limonene
210.07  linalool
220.10  linalyl acetate
150.07para- mentha-2,4(8)-diene
301.87alpha- muurolene
351.51alpha- muurolol
81.52  myrcene
130.33beta- ocimene
110.42beta- phellandrene
39.95alpha- pinene
51.20beta- pinene
60.30  sabinene
10.17  santene
330.24  spathulenol
240.39  terpinen-4-ol
90.13alpha- terpinene
120.23gamma- terpinene
280.10alpha- terpineol
162.15  terpinolene
20.38  tricyclene

M. Yatagai and T. Sato, Terpenes of leaf oils from conifers. Biochem. System. Ecol., 14, 469-478 (1986).

P&F 24, No. 3, 47, (1999)

pinus sylvestris leaf oil
Also in 1995, Stepen compared the composition of Pinus syIvestris oil produced in Siberia from needles harvested in July and September. He found that the oil varied as follows:
#%LeftshiftComponents
160.2-1.2beta- bisabolene
250.4-0.7  borneol
241.8-2.2iso borneol
261.1-3.2  bornyl acetate
45.3-7.0  camphene
212.1-2.9  camphor
73.4-11.6delta-3- carene
130.4-0.9beta- caryophyllene
200.1-0.2alpha- fenchol
181.6-1.9  fenchone
190.5iso fenchone
150.1-0.4alpha- humulene
86.1-8.7  limonene
120.3-0.9  longifolene
170.3-1.4alpha- muurolene
140.1-0.7epsilon- muurolene
64.6-5.9  myrcene
93.5-4.3beta- phellandrene
329.2-36.6alpha- pinene
52.2-4.2beta- pinene
11.8-3.4  santene
231.2-1.6  terpinen-4-ol
100.9-1.2gamma- terpinene
222.0-2.4alpha- terpineol
110.1-0.2  terpinolene
270.3-0.5alpha- terpinyl acetate
21.6-3.1  tricyclene

R. A. Stepen, The composition of essential oil and volatile terpenoids of Pinus sylvestris L. shoots in middle siberia. Rast. Resur., 31, 63-70 (1995).

P&F 26, No. 3, 66, (2001)

sandalwood oil east indian
#%LeftshiftComponents
150.10(Z)-(E)-alpha-bergamotal
30.12(E)-alpha- bergamotene
203.90(Z)-(E)-alpha-bergamotol
70.07beta- bisabolene
160.26alpha- bisabolol
130.64beta- bisabolol
100.26ar- curcumene
80.13beta- curcumene
60.04gamma- curcumene
180.38 dihydro-alpha-santalol
251.70(Z)- lanceol
120.06(E)- nerolidol
261.10(Z)- nuciferol
142.90alpha-santalal
90.07alpha-eka-santalal
170.56beta-santalal
110.01beta-eka-santalal
20.82alpha- santalene
51.40beta- santalene
40.97epi-beta- santalene
210.56(E)-alpha- santalol
241.50(E)-beta- santalol
1950.00(Z)-alpha- santalol
2320.90(Z)-beta- santalol
224.10epi-beta-santalol
10.01  santene
271.20  spirosantalol

E. J. Brunke and F. J. Hammerschmidt, Constituents of East Indian Sandalwood Oil—An Eighty Year Long “Stability Test.” Dragoco Rept., (4) 107-113 (1988).

P&F 16, No. 6, 49, (1991)

tagetes minuta flower oil rwanda
#%LeftshiftComponents
10.63  acetone
280.06  artemisyl ketone
33trace  bornyl acetate
34traceiso bornyl acetate
8trace  camphene
100.11delta-3- carene
160.041,8- cineole
21tracepara- cymene
221.03  dihydrotagetone
250.163,4- dimethyl octa-2,4,6-triene
70.02  ethyl 2-methyl butyrate
60.12  ethyl butyrate
150.032- hexenal
260.14(Z)-3- hexen-1-ol
141.77  limonene
320.17  linalool
230.54para- menth-4-en-3-one
20.034- methyl-2-pentanone
11trace1- methyl-3-isopropyl cyclohexane
130.11  myrcene
200.17(E)-beta- ocimene
1737.08(Z)-beta- ocimene
29trace(Z)-beta-ocimene epoxide
120.07alpha- phellandrene
360.082(10)-pinen-4-one
40.03alpha- pinene
90.28  sabinene
30.05  santene
386.31(E)- tagetenone
373.34(Z)- tagetenone
302.86(E)- tagetone
3135.40(Z)- tagetone
350.07  terpinen-4-ol
19tracegamma- terpinene
180.35  terpinolene
5tracealpha- thujene
270.022,4,6- trimethyl anisole
24trace1,7,7- trimethyl bicyclo(3.1.1)heptan-2-one

J. C. Chalchat, R. Ph. Garry and A. Muhayimana, Composition chimique d’huiles essentielles de Tagetes minuta L. du Rwanda. In: Valorisation dela Biomasse Végétale par les produits naturels. Edits., F-X. Garneau and G. J. Collin, p. 295-302, CRDI, Ottawa (1995).

P&F 25, No. 6, 32, (2000)

#%LeftshiftComponents
1trace  acetone
220.30  artemisyl ketone
27trace  bornyl acetate
28traceiso bornyl acetate
7trace  camphene
11tracedelta-3- carene
16trace1,8- cineole
190.30para- cymene
203.30  dihydrotagetone
6trace  ethyl 2-methyl butyrate
8trace  ethyl valerate
15trace2- hexenal
210.50(Z)-3- hexen-1-ol
141.30  limonene
26trace  linalool
13trace  myrcene
18trace(E)-beta- ocimene
1731.80(Z)-beta- ocimene
230.30(Z)-beta-ocimene epoxide
12tracealpha- phellandrene
3tracealpha- pinene
9tracebeta- pinene
50.50  propyl butyrate
100.30  sabinene
2trace  santene
301.80(E)- tagetenone
316.00(Z)- tagetenone
243.40(E)- tagetone
2546.00(Z)- tagetone
290.30  terpinen-4-ol
4tracealpha- thujene

J. C. Chalchat, R. Ph. Garry and A. Muhayimana, Composition chimique d’huiles essentielles de Tagetes minuta L. du Rwanda. In: Valorisation dela Biomasse Végétale par les produits naturels. Edits., F-X. Garneau and G. J. Collin, p. 295-302, CRDI, Ottawa (1995).

P&F 25, No. 6, 32, (2000)

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