BT

Typical G.C. analysis

carrot seed oil
#%LeftshiftComponents
360.08(E)- anethole
210.73(E)-alpha- bergamotene
201.08(Z)-alpha- bergamotene
380.23beta- bisabolene
430.21alpha- bisabolol
420.273- butyl phthalide
20.44  camphene
395.68  carotol
350.23  carvomenthone
153.56beta- caryophyllene
371.09  caryophyllene oxide
400.29 cedrene oxide
140.17alpha- copaene
100.41para- cymene
130.39  daucene
410.14  daucol
180.42alpha- farnesene
230.60beta- farnesene
310.89  geranial
3234.17  geranyl acetate
301.13alpha- humulene
70.48  limonene
120.11  linalool
191.24  longifolene
250.18para- mentha-1,3-dien-7-ol
51.87  myrcene
290.53  neral
331.01  nerol
81.92(E)-alpha- ocimene
19.09alpha- pinene
34.49beta- pinene
49.44  sabinene
340.14  sabinene hydrate
170.40alpha- santalene
220.67beta- santalene
440.13  sedanenolide
450.40  sedanolide (3-butyl-3a,4,5,6-tetrahydrophthalide)
280.44alpha- selinene
270.23beta- selinene
160.31  terpinen-4-ol
60.96alpha- terpinene
90.36gamma- terpinene
241.65alpha- terpineol
110.28  terpinolene
262.34  verbenol

F. Perineau, L. Ganou and A. Gaset, Etude de la production d’huile essentielle de fruit de carotte. Ind. Aliment. Agric., 108, 357-366 (1991).

P&F 17, No. 3, 61, (1992)

cedrus libanensis wood oil
#%LeftshiftComponents
350.80 atlantone
382.80(E)-alpha- atlantone
340.60(E)-gamma- atlantone
370.30(Z)-alpha- atlantone
360.60(Z)-beta-atlantone
330.40(Z)-gamma- atlantone
220.40(Z)-alpha- bisabolene
27>0.10alpha- calacorene
1>0.10  camphene
14>0.10  camphor
3>0.10delta-3- carene
170.20alpha- cedrene
211.40 chamigrene
7>0.10para- cymene
240.80alpha- dehydro-ar-himachalene
261.40gamma- dehydro-ar-himachalene
280.60oxido himachalene
9>0.10  fenchone
320.10  guaiazulene
10>0.10alpha- gurjunene
13>0.10beta- gurjunene
1814.20alpha- himachalene
2031.30beta- himachalene
196.90gamma- himachalene
300.50 himachalene oxide
292.20beta- himachalene oxide
5>0.10  limonene
310.80  longiborneol
160.50  longifolene
110.10alpha- longipinene
395.60  manool
2>0.104- methyl-3-penten-2-one
230.80 occidentalol acetate
150.10  sativene
4>0.10alpha- terpinene
6>0.10gamma- terpinene
8>0.10  terpinolene
250.40beta- vetivenene
12>0.10alpha- ylangene
J. of Ess. Oil Res. 12, No. 6, 763, (2000)
chamaecyparis obtusa leaf oil
#%LeftshiftComponents
131.23  borneol
177.15  bornyl acetate
361.70 cadin-10(15)-4-ol
272.76delta- cadinene
280.53gamma- cadinene
204.71beta-cadrene
300.41  calamenene
20.23  camphene
380.65  caryophylla-3,8(13)-dien-5alpha-ol
181.65(Z)- caryophyllene
190.28beta- caryophyllene
320.93  cedrol
250.48beta- cubebene
90.82para- cymene
211.47alpha- elemene
290.39gamma- elemene
3114.78  elemol
345.39alpha- eudesmol
356.54beta- eudesmol
338.28gamma- eudesmol
102.09alpha- fenchol
240.30beta- guaiene
63.05  limonene
120.41  longicyclene
370.73 longicyclenyl aclohol
150.72  longifolene
110.37alpha- longipinene
263.81alpha- muurolene
225.71gamma- muurolene
11.01alpha- pinene
42.77beta- pinene
31.61  sabinene
51.11alpha- terpinene
71.77gamma- terpinene
141.11alpha- terpineol
81.00  terpinolene
239.09alpha- terpinyl acetate
160.89  verbenone

B. Shieh, Y. Lizuka and Y. Matsubara, Monoterpenoid and sesquiterpenoid constituents of the essential oil of Hinoki (Chamaecyparis obtusa (Sieb. et Zucc. ) Endl.). Agric. Biol. Chem. (Japan), 45, 1497-1499 (1981).

P&F 8, No. 1, 61, (1983)

chamaecyparis obtusa root oil
#%LeftshiftComponents
120.54  borneol
170.65  bornyl acetate
321.18 cadin-1(10)-en-4alpha-ol
384.95 cadin-1(10)-en-4beta-ol
273.82delta- cadinene
282.12gamma- cadinene
395.28alpha- cadinol
355.88T- cadinol
200.68beta-cadrene
291.55  calamenene
20.50  camphene
421.26  caryophylla-3,8(13)-dien-5alpha-ol
180.55(Z)- caryophyllene
190.52beta- caryophyllene
302.61beta- caryophyllene alcohol
160.40  copaene
80.53para- cymene
210.44alpha- elemene
90.71alpha- fenchol
250.39alpha- guaiene
220.39alpha- humulene
50.55  limonene
4019.73 longi-alpha-nojigiku alcohol
338.43 longi-beta-camphenilan aldehyde
110.65  longicyclene
414.84 longicyclenyl aclohol
140.64  longifolene
362.15 longiisohomocamphenilone
100.48alpha- longipinene
311.27 longiverbanol
346.23 longiverbanone
261.71alpha- muurolene
230.84gamma- muurolene
374.53T- muurolol
10.73alpha- pinene
30.61beta- pinene
40.41alpha- terpinene
60.45gamma- terpinene
133.53alpha- terpineol
70.50  terpinolene
240.79alpha- terpinyl acetate
152.44  verbenone

B. Shieh, Y. Lizuka and Y. Matsubara, Monoterpenoid and sesquiterpenoid constituents of the essential oil of Hinoki (Chamaecyparis obtusa (Sieb. et Zucc. ) Endl.). Agric. Biol. Chem. (Japan), 45, 1497-1499 (1981).

P&F 8, No. 1, 61, (1983)

chamaecyparis obtusa wood oil
#%LeftshiftComponents
120.33  borneol
170.40  bornyl acetate
310.97 cadin-1(10)-en-4alpha-ol
346.76 cadin-1(10)-en-4beta-ol
2710.82delta- cadinene
2812.47gamma- cadinene
3520.51alpha- cadinol
3210.61T- cadinol
200.07beta-cadrene
290.03  calamenene
20.18  camphene
370.83  caryophylla-3,8(13)-dien-5alpha-ol
180.12(Z)- caryophyllene
190.05beta- caryophyllene
301.49beta- caryophyllene alcohol
160.06  copaene
80.22para- cymene
210.04alpha- elemene
90.42alpha- fenchol
250.12alpha- guaiene
220.03alpha- humulene
50.21  limonene
110.05  longicyclene
360.94 longicyclenyl aclohol
140.61  longifolene
100.10alpha- longipinene
265.78alpha- muurolene
231.65gamma- muurolene
3316.44T- muurolol
10.44alpha- pinene
30.21beta- pinene
40.15alpha- terpinene
60.15gamma- terpinene
130.14alpha- terpineol
70.19  terpinolene
240.19alpha- terpinyl acetate
150.29  verbenone

B. Shieh, Y. Lizuka and Y. Matsubara, Monoterpenoid and sesquiterpenoid constituents of the essential oil of Hinoki (Chamaecyparis obtusa (Sieb. et Zucc. ) Endl.). Agric. Biol. Chem. (Japan), 45, 1497-1499 (1981).

P&F 8, No. 1, 61, (1983)

lippia citriodora oil
#%LeftshiftComponents
460.5allo- aromadendrene
280.4  bornyl butyrate
430.8beta- bourbonene
480.1delta- cadinene
500.6gamma- cadinene
590.9T- cadinol
410.1  carvacrol
320.4trans- carveol
400.8  carvone
450.4beta- caryophyllene
52traceiso caryophyllene
555.5  caryophyllene oxide
581.0iso caryophyllene oxide
530.4alpha- cedrene
1412.41,8- cineole
420.6alpha- copaene
470.6beta- cubebene
51trace  cuparene
494.6ar- curcumene
70.2para- cymene
360.6  fenchone
269.9  geranial
350.7  geranic acid
330.5  geraniol
291.6  geranyl acetate
300.9  geranyl isobutyrate
310.3  geranyl propionate
440.1alpha- gurjunene
130.4(Z)-3- hexen-1-yl butyrate
120.3  hexyl 2-methyl butyrate
43.7  limonene
191.3  linalool
180.1(E)- linalool oxide furanoid
17trace(Z)- linalool oxide furanoid
540.2  longifolene
240.7  methyl geranate
97.46- methyl-5-hepten-2-one
560.5alpha- muurolol
370.2  myrtenal
236.9  neral
571.2  nerolidol
270.6  neryl acetate
100.33- octanol
110.71- octen-3-ol
5tracealpha- phellandrene
11.4alpha- pinene
20.3beta- pinene
390.7trans- pinocarveol
210.7iso pulegol
15trace rose oxide
30.2  sabinene
380.6(E)- sabinene hydrate
200.3(Z)- sabinene hydrate
605.2  spathulenol
221.0  terpinen-4-ol
61.0gamma- terpinene
252.3alpha- terpineol
8trace  terpinolene
160.3alpha- thujone
340.3  thymol
610.1  viridiflorol

J. Bellakhdar, A.IL. Idrissi, S. Canigueral, J. Iglesias and R.Vila, Analysis de L'huile essentielle dela verveine odorante (Lippia citriodora H, B, and K). Plant. Medicin Phytother., 26, 269-273 (1993).

P&F 23, No. 5, 55, (1998)

pelargonium capitatum l. l'hér. ex aiton oil cuba
#%LeftshiftComponents
50.10  borneol
150.80beta- bourbonene
282.40alpha- bulnesene
471.00  cadalene
290.10gamma- cadinene
322.60delta- cadinene
450.20alpha- cadinol
340.30alpha- calacorene
350.10beta- calacorene
310.20(Z)- calamenene
183.20beta- caryophyllene
3814.70  caryophyllene oxide
825.60  citronellol
120.10  citronellyl acetate
102.50  citronellyl formate
140.20alpha- copaene
130.10alpha- cubebene
300.60  cubebol
430.60  cubenol
160.70beta- elemene
530.80  ethyl hexadecanoate
203.00(Z)-beta- farnesene
490.40(Z,E)- farnesol
510.20(E,E)- farnesol
520.40(Z,E)- farnesyl acetate
91.90  geraniol
360.10  geranyl butyrate
230.30  geranyl propionate
251.80  germacrene D
390.10  gleenol
197.20alpha- guaiene
270.20(Z)-beta- guaiene
210.70alpha- humulene
401.80  humulene oxide II
460.5014- hydroxy-9-epi-beta-caryophyllene
410.40(E)-sesqui lavandulol
10.10  linalool
170.10  longifolene
40.30iso menthone
240.10gamma- muurolene
420.40epi-alpha- muurolol
500.40(E)- nerolidol acetate
480.90(Z)- nerolidyl acetate
220.60alpha- patchoulene
25.50(Z)- rose oxide
34.50(E)- rose oxide
440.40  selin-11-en-4alpha-ol
260.30beta- selinene
372.00  spathulenol
60.40  terpinen-4-ol
70.20alpha- terpineol
110.10  thymol
333.60 unknown MW 218
J. of Ess. Oil Res. 13, No. 1, 21, (2001)
pinus sylvestris leaf oil
Also in 1995, Stepen compared the composition of Pinus syIvestris oil produced in Siberia from needles harvested in July and September. He found that the oil varied as follows:
#%LeftshiftComponents
160.2-1.2beta- bisabolene
250.4-0.7  borneol
241.8-2.2iso borneol
261.1-3.2  bornyl acetate
45.3-7.0  camphene
212.1-2.9  camphor
73.4-11.6delta-3- carene
130.4-0.9beta- caryophyllene
200.1-0.2alpha- fenchol
181.6-1.9  fenchone
190.5iso fenchone
150.1-0.4alpha- humulene
86.1-8.7  limonene
120.3-0.9  longifolene
170.3-1.4alpha- muurolene
140.1-0.7epsilon- muurolene
64.6-5.9  myrcene
93.5-4.3beta- phellandrene
329.2-36.6alpha- pinene
52.2-4.2beta- pinene
11.8-3.4  santene
231.2-1.6  terpinen-4-ol
100.9-1.2gamma- terpinene
222.0-2.4alpha- terpineol
110.1-0.2  terpinolene
270.3-0.5alpha- terpinyl acetate
21.6-3.1  tricyclene

R. A. Stepen, The composition of essential oil and volatile terpenoids of Pinus sylvestris L. shoots in middle siberia. Rast. Resur., 31, 63-70 (1995).

P&F 26, No. 3, 66, (2001)

pinus sylvestris leaf oil estonia
The following year, Orav et al. (1996) analyzed an oil of Estonian P sylvestris needle oil. Using a combination of CC and CC/MS they determined that the oil was coin prised of the following constituents:
#%LeftshiftComponents
280.20  bicyclogermacrene
150.30  borneol
241.80  bornyl acetate
410.10beta- bourbonene
380.10a cadinene
364.80delta- cadinene
341.20gamma- cadinene
482.70alpha- cadinol
330.20  calamenene
63.40  camphene
13trace  camphor
1623.70delta-3- carene
432.90beta- caryophyllene
424.90  caryophyllene oxide
21trace  citronellol
350.10alpha- copaene
450.10beta- copaene
200.10para- cymene
390.30beta- elemene
310.80alpha- farnesene
400.20beta- farnesene
22trace  geraniol
32trace geranyl acetate + alpha-ylangene
230.10alpha- guaiene
470.50alpha- humulene
50.80  limonene
370.10  longifolene
302.80alpha- muurolene
272.00gamma- muurolene
250.30epsilon-muurolene + beta-guaiene
461.00T- muurolol
440.70alpha-muurolol + T-cadinol
122.10  myrcene
29trace neryl acetate + alpha-cubebene
71.50(E)-beta- ocimene
140.20alpha- phellandrene
21.00beta-phellandrene + 1,8-cineole
428.10alpha- pinene
102.10beta- pinene
81.00  sabinene
170.40  terpinen-4-ol
180.20alpha- terpinene
90.30gamma- terpinene
190.10alpha- terpineol
112.60  terpinolene
260.60alpha-terpinyl acetate + delta-elemene
30.20alpha- thujene
10.70  tricyclene

A. Orav, T. Kalias and M. Liiv, Analysis of terpenoic composition of conifer needle oils by steam distillation/extraction gas chromatography and gas chromatography-mass spectrometry. Chromatographia, 43, 215-219 (1996).

P&F 26, No. 3, 66, (2001)

pinus sylvestris leaf oil yugoslavia
Scots pine needle oil of Yugoslavian origin was deter mined by Ruzic et al. (1999) to contain the following constituents:
#%LeftshiftComponents
130.10  borneol
33.60  camphene
71.10delta-3- carene
181.20beta- caryophyllene
160.10  citronellol
90.20para- cymene
190.40  germacrene D
1023.90 limonene + beta-phellandrene
170.10  longifolene
150.90 longipinene
64.80  myrcene
240.30alpha- pinene
515.70beta- pinene
40.20  sabinene
80.20alpha- terpinene
110.20gamma- terpinene
140.40alpha- terpineol
120.60  terpinolene
10.70  tricyclene

N. J. Ruzic, S. S. Petrovic, T. Stevanovic-Janezic and S. D. Petrovic, Optimization of the preparation of the essential oil from technical foliage of white pine (Pinus sylvestris L.) by steam distillation, Hem. Innd., 53, 231-234 (1999).

P&F 26, No. 3, 66, (2001)

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